All submissions of the EM system will be redirected to Online Manuscript Submission System. Authors are requested to submit articles directly to Online Manuscript Submission System of respective journal.
Abstract
Development and validation of HPLC method for the determination of pregabalin in capsules Highly accessed article
Author(s): GB Kasawar, MN Farooqui
Dr. Rafi q Zakaria Campus, Post Graduate Studies and Research Centre, Moulana Azad College Rouza Bagh, Aurangabad-431 00, India
Correspondence Address:
E-mail: mazahar_64@rediffmail.com
Dr. Rafi q Zakaria Campus, Post Graduate Studies and Research Centre, Moulana Azad College Rouza Bagh, Aurangabad-431 00, India
Correspondence Address:
E-mail: mazahar_64@rediffmail.com
A simple, precise, specifi c, and accurate reverse phase HPLC method has been developed for the determination of pregabalin in capsule dosage form. The chromatography was set on Hypersil BDS, C8, 150×4.6 mm, 5 μm column using photodiode array detector. The mobile phase consisting of phosphate buffer pH 6.9 and acetonitrile in the ratio of 95:05 with fl ow rate of 1 ml/min. The method was validated according to ICH guidelines with respect to specifi city, linearity, accuracy, precision and robustness. Lower limit of quantifi cation is 0.6 mg/l. The pregabalin sample solution was found to be stable at room temperature for about 26 h.
hd hindi xxx video, www qorno com, muslim sex video, ove sex video, beautiful indian bhabhi fukad hard by devar, new hd xxx videos
Full-Text | PDF